HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 18626180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Ethyl-3-nitrobenzoic acid | HCID 8167086 | — |
| Product | HCID 18626180 | HCID 18626180 | 74% |
Reaction Steps
Prepared according to the procedure described for Example 1 using oxalyl chloride (2.0 mL, 22.93 mmol), 3-nitro-4-ethylbenzoic acid (4.00 g, 20.51 mmol), DMF (1.0 mL, 12.92 mmol), and aniline (3.8 mL, 41.70 mmol) to afford the 5 product (4.1 g); m.p. 111-113° C. after trituration in hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-6c88ead14ee943bea76f30fc886d0076 |
| Source note | uspto-grants-2003_03 |