HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 18626168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Reactant | 3,5-Dichlorobenzaldehyde | HCID 35746 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Product | HCID 18626168 | HCID 18626168 | 32.4% |
Reaction Steps
Prepared according to the procedure of Example 50 using 3,5-dichloro-benzaldehyde (0.88 g, 5.0 mmol), 3-amino-4-methoxy-N-phenyl-benzamide (1.22 g, 5.0 mmol), acetic acid (0.24 g, 5.3 mmol), and sodium triacetoxyborohydride (1.12 mmol) to afford the product (0.65 g); m.p. 164-165° C. after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-d3c899898ded4a3197861d8ea47b88b6 |
| Source note | uspto-grants-2003_03 |