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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1859673Generated: October 31, 2026

Acetic Acid → HCID 18626090, compound

https://huagongshe.com/reaction/1859673

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantVeratraldehydeHCID 8419—
Reactant3-Amino-4-methoxybenzanilideHCID 8426—
ReactantSodium triacetoxyborohydrideHCID 5049666—
ProductHCID 18626090HCID 1862609063.7%

Reaction Steps

Prepared according to the procedure of Example 50 using 3,4-dimethoxybenzaldehyde (1.94 g, 11.6 mmol), 3-amino-4-methoxy-N-phenyl-benzamide (2.8 g, 11.6 mmol), acetic acid (0.69 g, 11.5 mmol), and sodium triacetoxyborohydride (2.6 g, 11.7 mmol) to afford the product (2.9 g); m.p. 187-188° C. after recrystallization from ethanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06528528B2
Source datasetuspto-grants-2003_03
ORD IDord-0432b81d4b7c4bba9d1615c8b92c0318
Source noteuspto-grants-2003_03