HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenyl isothiocyanate → HCID 54524796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenyl isothiocyanate | HCID 138776 | — |
| Reactant | 3-Amino-4-methyl-N-phenylbenzamide | HCID 12607981 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54524796 | HCID 54524796 | 84.7% |
Reaction Steps
Prepared according to the procedure described for Example 60 using of 3-amino-4-methyl-N-phenyl-benzamide (0.5 g, 2.2 mmol) and 3,5-dichlorophenyl isothiocyanate (0.458 g, 2.2 mmol). Trituration in ethyl acetate afforded the product (0.802 g) in two crops; m.p. 182-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-9ec160d1796948f784b7d07258ce0105 |
| Source note | uspto-grants-2003_03 |