HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenyl isothiocyanate → HCID 54283304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenyl isothiocyanate | HCID 138776 | — |
| Reactant | HCID 18626123 | HCID 18626123 | — |
| Product | HCID 54283304 | HCID 54283304 | 49.6% |
Reaction Steps
Prepared according to the procedure described for Example 60 using 3-amino-4-fluoro-N-phenyl-benzamide from Example 9 (0.481 g, 2.09 mmol) and 3,5-dichlorophenyl isothiocyanate (0.427 g , 2.09 mmol). Filtration afforded the product (0.45 g) in two crops; m.p. 173-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-058f2e885dab47a783bd5b41f7d282c6 |
| Source note | uspto-grants-2003_03 |