HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenyl isothiocyanate → HCID 18626209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenyl isothiocyanate | HCID 138776 | — |
| Reactant | 3-Amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide | HCID 9948627 | — |
| Product | HCID 18626209 | HCID 18626209 | 50.4% |
Reaction Steps
Prepared according to the procedure described for Example 78 using 3-amino-4-methoxy-N-(3,4-dichloro-phenyl)-benzamide from Example 4 (0.932 g, 3.00 mmol) and 3,5-dichlorophenyl isothiocyanate (0.335 g, 1.64 mmol). After 2 days, filtration afforded the product (0.426 g); m.p. 189-191° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-673c403691194f3a9d1c8cd1481aa47a |
| Source note | uspto-grants-2003_03 |