HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenyl isothiocyanate → HCID 17921779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenyl isothiocyanate | HCID 15241 | — |
| Reactant | HCID 16791679 | HCID 16791679 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 17921779 | HCID 17921779 | 89.7% |
Reaction Steps
Prepared according to the procedure described for Example 100 using 3-amino-N-(3-chlorophenyl)4-methoxy-benzamide from Example 16 (0.5545 g, 2.01 mmol) and 4-fluorophenyl isothiocyanate (0.3073 g, 2.01 mmol), and omitting the trituration in methanol to afford the product (0.775 g); m.p. 184-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-dc33966b18d64008b7e000bf1bf33893 |
| Source note | uspto-grants-2003_03 |