Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Amino-4-methoxybenzanilide → 3-(Quinoline-8-sulfonylamino)-4-methoxy-N-phenyl-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| 반응물 | 8-Quinolinesulfonyl chloride | HCID 29220 | — |
| 생성물 | 3-(Quinoline-8-sulfonylamino)-4-methoxy-N-phenyl-benzamide | HCID 9824185 | 76.9% |
반응 단계
Prepared according to the procedure described for Example 126 using 8-quinolinesulfonyl chloride (0.68 g, 3.0 mmol) and 3-amino-4-methoxy-N-phenyl-benzamide (0.73 g, 3.0 mmol) to afford the product (1.0 g); m.p. 187-188° C. after trituration in diethyl ether and recrystallization from ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06528528B2 |
| 출처 데이터셋 | uspto-grants-2003_03 |
| ORD ID | ord-f2c2851b433a43a781b0f35572070877 |
| 출처 메모 | uspto-grants-2003_03 |