HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-4-methoxybenzanilide → HCID 54168795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Reactant | Phenylmethanesulfonyl chloride | HCID 74740 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54168795 | HCID 54168795 | 63.1% |
Reaction Steps
Prepared according to the procedure described for Example 121 using benzylsulfonyl chloride (1.90 g, 10 mmol), 3-amino-4-methoxy-N-phenyl-benzamide (2.43 g, 10 mmol), and pyridine (25 mL) to afford the product (2.5 g); m.p. 216-216° C. after trituration in hexanes/ethyl acetate (1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-1b787f2fe6d94f27ac32f393de179922 |
| Source note | uspto-grants-2003_03 |