HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 10686697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-Nitro-4-(trifluoromethoxy)benzoic acid | HCID 18626217 | — |
| Product | HCID 10686697 | HCID 10686697 | 88.5% |
Reaction Steps
Prepared according to the procedure described for Example 1 using 3-nitro-4-trifluoromethoxybenzoic acid from Step A (5.1 g, 20.5 mmol), oxalyl chloride (2.1 mL, 20.5 mmol), and 4-fluoroaniline (Aldrich, Milwaukee, Wis.) (4.6 g, 41.1 mmol) to afford the product (5.7 g); m.p. 139-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-e040940dff554a77baaffd2d70bd61f5 |
| Source note | uspto-grants-2003_03 |