HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Furaldehyde → HCID 54077791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Furaldehyde | HCID 10351 | — |
| Reactant | 6-(2-Imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-one | HCID 15486912 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | HCID 54077791 | HCID 54077791 | 70% |
Reaction Steps
According to the method of Example 8, 6-(2-imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-one (0.20 g, 0.78 mmol) was reacted with 3-furaldehyde (0.083 g, 0.86 mmol) in 2 mL of 4% KOH in EtOH for 48 hours at room temperature to afford 0.182 g (70%) of the title compound, mp 116-117° C.: APCI-MS m/e 335.3 M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528535B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-0fbbdbb64ddf4d7e971adead1918b99c |
| Source note | uspto-grants-2003_03 |