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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1859786Generated: October 31, 2026

3-Furaldehyde → HCID 54077791, compound

https://huagongshe.com/reaction/1859786

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-FuraldehydeHCID 10351—
Reactant6-(2-Imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-oneHCID 15486912—
SolventEthanolHCID 702—
SolventPotassium HydroxideHCID 14797—
ProductHCID 54077791HCID 5407779170%

Reaction Steps

According to the method of Example 8, 6-(2-imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-one (0.20 g, 0.78 mmol) was reacted with 3-furaldehyde (0.083 g, 0.86 mmol) in 2 mL of 4% KOH in EtOH for 48 hours at room temperature to afford 0.182 g (70%) of the title compound, mp 116-117° C.: APCI-MS m/e 335.3 M++1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06528535B2
Source datasetuspto-grants-2003_03
ORD IDord-0fbbdbb64ddf4d7e971adead1918b99c
Source noteuspto-grants-2003_03