HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinaldic Acid → 1,2,3,4-Tetrahydroquinoline-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinaldic Acid | HCID 7124 | — |
| Reactant | D-Psicose | HCID 441036 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1,2,3,4-Tetrahydroquinoline-2-carboxylic acid | HCID 12877794 | — |
Reaction Steps
A mixture of PtO2 (25 wt. %) and 2-quinolinecarboxylic acid (Aldrich) in acetic acid was hydrogenated at RT under 60 Psi overnight. The reaction mixture was stripped to dryness to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528505B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-516ff1338af64bab9d9ac21590039e5f |
| Source note | uspto-grants-2003_03 |