HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dinitrophenol → 1-(2-Ethoxy-ethoxy)-2,3-dinitro-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dinitrophenol | HCID 6191 | — |
| Reactant | Ethane, 1-chloro-2-ethoxy- | HCID 12341 | — |
| Product | 1-(2-Ethoxy-ethoxy)-2,3-dinitro-benzene | HCID 86761133 | — |
Reaction Steps
1-(2-Ethoxy-ethoxy)-2,3-dinitro-benzene was prepared by a procedure according to example 108 (i) starting from 500 mg (2.72 mmol) 2,3-dinitro-phenol and 0.72 mL (6.52 mmol) 1-chloro-2-ethoxy-ethane. Yield: 450 mg MS (ES+): m/e=257.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07741341B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-c6240d9049d04e7597bd4c2718148baa |
| Source note | uspto-grants-2010_06 |