HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18625713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(2-Bromoethoxy)tetrahydro-2H-pyran | HCID 86621 | — |
| Reactant | HCID 18625931 | HCID 18625931 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18625713 | HCID 18625713 | 100.1% |
Reaction Steps
In a similar manner to that described in Reference example 3(e), a reaction was carried out using ethyl 3-(4-hydroxyphenyl)-2-(4-isopropylphenoxy)propionate (14.8 g), which is the product of Reference example 5(d), 2-(2-bromoethoxy)tetrahydropyran (28.2 g) and potassium carbonate (24.9 g) in dimethylformamide and the reaction mixture was treated to afford the desired compound (20.6 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-97410f526ec542ae989f35aef6124f27 |
| Source note | uspto-grants-2003_03 |