HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → Ethyl 3-[4-(2-azidoethoxy)phenyl]-2-butylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Ethyl 2-butyl-3-[4-(2-methanesulfonyloxyethoxy)phenyl]propionate | HCID 18625769 | — |
| Product | Ethyl 3-[4-(2-azidoethoxy)phenyl]-2-butylpropionate | HCID 18625797 | 114.5% |
Reaction Steps
In a similar manner to that described in Reference example 3(h), a reaction was carried out using ethyl 2-butyl-3-[4-(2-methanesulfonyloxyethoxy)phenyl]propionate (1.65 g), which is the product of Reference example 6(f), and sodium azide (0.95 g) and the reaction mixture was treated to afford the desired compound (1.62 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-4a235c9f9ce14c91a9b8bb5369b909ad |
| Source note | uspto-grants-2003_03 |