HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-[4-(2-azidoethoxy)phenyl]-2-butylpropionate → Ethyl 3-[4-(2-aminoethoxy)phenyl]-2-butylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-[4-(2-azidoethoxy)phenyl]-2-butylpropionate | HCID 18625797 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Ethyl 3-[4-(2-aminoethoxy)phenyl]-2-butylpropionate | HCID 18625891 | 100.1% |
Reaction Steps
In a similar manner to that described in Reference example 1(d), a reaction was carried out using ethyl 3-[4-(2-azidoethoxy)phenyl]-2-butylpropionate (1.62 g), which is the product of Reference example 6(g), and palladium on carbon (5%, 243 mg) and the reaction mixture was treated to afford the title compound (1.49 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-f5db709fd7a74417b479f64d13a29e17 |
| Source note | uspto-grants-2003_03 |