HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(4-benzyloxybenzyl)-2-methylcaproate → Ethyl 2-butyl-3-(4-hydroxyphenyl)-2-methylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(4-benzyloxybenzyl)-2-methylcaproate | HCID 18625782 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Ethyl 2-butyl-3-(4-hydroxyphenyl)-2-methylpropionate | HCID 18625949 | 100.1% |
Reaction Steps
In a similar manner to that described in Reference example 1(d), a reaction was carried out using ethyl 2-(4-benzyloxybenzyl)-2-methylcaproate (3.95 g), which is the product of Reference example 10(a), and palladium on carbon (5%, 0.40 g) and the reaction mixture was treated to afford the desired compound (2.95 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-d5310086a6344bf8aa2cfc9f91efa524 |
| Source note | uspto-grants-2003_03 |