Sodium Azide → Ethyl 3-[4-(2-azidoethoxy)phenyl]-2-butyl-2-methylpropionate

Participants

Reaction Steps

In a similar manner to that described in Reference example 3(h), a reaction was carried out using ethyl 2-butyl-3-[4-(2-methanesulfonyloxyethoxy)phenyl]-2-methylpropionate (3.17 g), which is the product of Reference example 10(e), and sodium azide (1.60 g) and the reaction mixture was treated to afford the desired compound (2.80 g) as a syrup.

Provenance & Evidence