HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69877110, compound → HCID 69876585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69877110 | HCID 69877110 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69876585 | HCID 69876585 | 90.9% |
Reaction Steps
In a similar manner to that described in Reference example 1(d), a reaction was carried out using (S)-4-benzyl-3-[(2S,3R)-3-(4-benzyloxyphenyl)-3-hydroxy-2-(4-isopropylphenoxy)propionyl]oxazolidine-2-one (25.0 g), which is the product of Reference example 29(b) and palladium on carbon (5%, 2.50 g) and the reaction mixture was treated to afford the desired compound (19.1 g) as a mass of foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-4d022058b5ed412f9ef20a233c162bb2 |
| Source note | uspto-grants-2003_03 |