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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1860043Generated: November 1, 2026

Potassium Carbonate → HCID 86758864, compound

https://huagongshe.com/reaction/1860043

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactanttert-Butyl N-(2-((methylsulfonyl)oxy)ethyl)carbamateHCID 22605302—
ReactantHCID 54265940HCID 54265940—
ProductHCID 86758864HCID 8675886491.2%

Reaction Steps

In a similar manner to that described in Reference example 25, a reaction was carried out using 2-trimethylsilylethyl (S)-3-(4-hydroxyphenyl)-2-(4-isopropylphenoxy)propionate (4.80 g), which is the product of Reference example 29(e), t-butyl 2-methanesulfonyloxyethylcarbamate (7.17 g) and potassium carbonate (8.28 g) and the reaction mixture was treated to afford the desired compound (5.94 g) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06528525B1
Source datasetuspto-grants-2003_03
ORD IDord-4abdae7f3d0140cd8638bc355209ccb0
Source noteuspto-grants-2003_03