HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86758865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | tert-Butyl N-(2-((methylsulfonyl)oxy)ethyl)carbamate | HCID 22605302 | — |
| Reactant | HCID 54265939 | HCID 54265939 | — |
| Product | HCID 86758865 | HCID 86758865 | 88% |
Reaction Steps
In a similar manner to that described in Reference example 25, a reaction was carried out using 2-trimethylsilylethyl (R)-3-(4-hydroxyphenyl)-2-(4-isopropylphenoxy)propionate (221 mg), which is the product of Reference example 30(e), t-butyl 2-methanesulfonyloxyethylcarbamate (330 mg) and potassium carbonate (381 mg) and the reaction mixture was treated to afford the desired compound (264 mg) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-70e96bba93f240acbcfe73af63dc10fb |
| Source note | uspto-grants-2003_03 |