HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 18625893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18625984 | HCID 18625984 | — |
| Reactant | HCID 86758867 | HCID 86758867 | — |
| Product | HCID 18625893 | HCID 18625893 | 133% |
Reaction Steps
In a similar manner to that described in Reference example 2(a), a reaction was carried out using 4-[3-(4-pyridine-2-ylbenzoylamino)propyl]benzylchloride (488 mg), which is the product of Reference example 50(c), sodium hydride (55% suspension in oil, 64 mg) and benzyl (3-phenylpropyl)malonate (540 mg) and the reaction mixture was treated to afford the title compound (0.65 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-0e295a40f2f945b79931a638e769c21c |
| Source note | uspto-grants-2003_03 |