Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1860099Generated: October 31, 2026

Potassium Carbonate → HCID 86590722, compound

https://huagongshe.com/reaction/1860099

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantN-[(Phenylmethoxy)carbonyl]-L-tyrosine methyl esterHCID 7010613—
Reactanttert-Butyl N-(2-((methylsulfonyl)oxy)ethyl)carbamateHCID 22605302—
ProductHCID 86590722HCID 8659072246.8%

Reaction Steps

In a similar manner to that described in Reference example 25, a reaction was carried out using N-benzyloxycarbonyl-L-tyrosine methyl ester (4.94 g), t-butyl 2-methanesulfonyloxyethylcarbamate (8.97 g) and potassium carbonate (10.4 g) and the reaction mixture was treated to afford the title compound (3.32 g) as colorless crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06528525B1
Source datasetuspto-grants-2003_03
ORD IDord-d3a2f958240241d2b2c833f8388e52ec
Source noteuspto-grants-2003_03