反应详情

温度

110 °C

A mixture of ethyl 3-(4-benzyloxyphenyl)-2-methanesulfonyloxypropionate (4.00 g) and aniline (5 ml) was stirred at 110° C. for 24 hours. The reaction mixture was purified via chromatography on silica gel column using ethyl acetate/hexane=1/4 as the eluant to afford the desired compound (3.94 g) as a syrup.

1. customThe reaction mixture was purified via chromatography on silica gel column