HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Anisoyl chloride → HCID 18627805, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Anisoyl chloride | HCID 74374 | — |
| Reactant | (+-)-1-Aminoindan | HCID 123445 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 18627805 | HCID 18627805 | — |
Reaction Steps
The title compound was prepared from (rac)-1-aminoindan (1.6 g, 12.3 mmole) and m-anisoyl chloride (1.9 g, 13.54 mmole) as in Ex. 46; crystallization from EtOAc:hexane gave 2.0 g (7.2 mmole, 59%) white solid, mp: 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528685B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-69d8b4cdb72c4fd59d0eb2081da77b08 |
| Source note | uspto-grants-2003_03 |