HRID1860393

反应详情

EQUATION

反应方程式

HRID 1860393 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

1-[2-(4-methoxyphenyl)ethoxy]-2,3-epoxypropane (24.1). By condensation of 4.8 g (31.5 mmol) of 4-methoxyphenethyl alcohol in a mixture of 25 ml of epichlorohydrin and 18 ml of 50% caustic soda and 430 mg of Bu4NHSO4 according to process 23.1, 4.42 g (yield: 67%) of glycidyl ether of formula 24.1 are prepared: