Pyridine N-Oxide → HCID 178500191, compound

HRID 1860633Notes

Reaction equation

HRID 1860633 reaction equation
C(O[C:6]([NH:8][C:9]1[N:14]=[C:13]([CH2:15][CH2:16][O:17][C:18]2[CH:23]=[CH:22][C:21]([CH2:24][C:25]([CH3:32])([CH3:31])[CH2:26][C:27]([O:29][CH3:30])=[O:28])=[CH:20][CH:19]=2)[CH:12]=[CH:11][CH:10]=1)=O)(C)(C)C.[N+]1([O-:39])C=CC=CC=1>>[CH3:31][C:25]([CH3:32])([CH2:24][C:21]1[CH:22]=[CH:23][C:18]([O:17][CH2:16][CH2:15][CH2:13][NH:14][C:9]2[CH:10]=[CH:11][CH:12]=[CH:6][N+:8]=2[O-:39])=[CH:19][CH:20]=1)[CH2:26][C:27]([O:29][CH3:30])=[O:28]

Participants

3

Reactant 2

HCID 12753Pyridine N-OxideHCID 12018747HCID 12018747, compound

Product 1

HCID 178500191HCID 178500191, compound

Procedure

The procedure for the preparation of the product of STEP 7, EXAMPLE 4 was repeated using 2-[3-hydroxy-1-propyl)amino]pyridine-N-oxide (Ref: WO 98/30542) in the place of the product of STEP 6, EXAMPLE 4 to provide the above product as a colorless gum.

Sources & evidence

ORD record
ord-5a331e119488439690151687f1537439
Source dataset
uspto-grants-2003_03
Patent number
US06531494B1

Reaction notes

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