HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → HCID 12017316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | HCID 178500191 | HCID 178500191 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 12017316 | HCID 12017316 | — |
Reaction Steps
A mixture of the product of STEP 1 (0.95 g), cyclohexene (Aldrich, 7 mL), 10% Pd/C (0.2 g) and isopropanol (10 mL) was heated to reflux for 20 hours. The mixture was filtered through celite and concentrated in vacuo. The residue was purified by chromatography using ethyl acetate as eluant to provide the above product as a thick gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06531494B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-71ef0dd20326412b9bbd445b140cde29 |
| Source note | uspto-grants-2003_03 |