3,4-Dimethoxybenzeneacetonitrile → HCID 54478485, compound

HRID 1861577Notes

Reaction equation

HRID 1861577 reaction equation
[CH3:1][O:2][C:3]1[C:10]([O:11][CH3:12])=[C:9]([O:13][CH3:14])[CH:8]=[CH:7][C:4]=1[CH:5]=O.[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH2:25][C:26]#[N:27])[CH:20]=[CH:21][C:22]=1[O:23][CH3:24]>>[CH3:15][O:16][C:17]1[CH:18]=[C:19]([C:25](=[CH:5][C:4]2[CH:7]=[CH:8][C:9]([O:13][CH3:14])=[C:10]([O:11][CH3:12])[C:3]=2[O:2][CH3:1])[C:26]#[N:27])[CH:20]=[CH:21][C:22]=1[O:23][CH3:24]

Participants

3

Reactant 2

HCID 667273,4-DimethoxybenzeneacetonitrileHCID 750062,3,4-Trimethoxybenzaldehyde

Product 1

HCID 54478485HCID 54478485, compoundYield 90%

Procedure

Following the Procedure A, the reaction was performed with 1.96 g of 2,3,4-trimethoxybenzaldehyde (10 mmol) and 1.77 g 3,4-dimethoxyphenyl-acetonitrile (10 mmol), affording 2-(3,4-dimethoxy-phenyl)-3-(2,3,4-trimethoxy-phenyl)-acrylonitrile as yellow powder (yield 3.2 g, 90%).

Sources & evidence

ORD record
ord-8a63f9a78815443cbc745d6ceaf795f6
Source dataset
uspto-grants-2003_03
Patent number
US06534135B1

Reaction notes

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