HCID 18621003, compound → HCID 18620727, compound

HRID 1861711Notes

Reaction equation

HRID 1861711 reaction equation
[C:1]([N:4]1[CH2:9][CH2:8][CH:7]([CH2:10][CH2:11][CH2:12][CH2:13][C:14]([OH:16])=O)[CH2:6][CH2:5]1)(=[O:3])[CH3:2].[C:17]([N:20]1[CH2:26][CH2:25][C:24]2[CH:27]=[CH:28][CH:29]=[CH:30][C:23]=2[CH2:22][CH2:21]1)(=[O:19])[CH3:18]>>[C:1]([N:4]1[CH2:5][CH2:6][CH:7]([CH2:10][CH2:11][CH2:12][CH2:13][C:14]([C:29]2[CH:28]=[CH:27][C:24]3[CH2:25][CH2:26][N:20]([C:17](=[O:19])[CH3:18])[CH2:21][CH2:22][C:23]=3[CH:30]=2)=[O:16])[CH2:8][CH2:9]1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 18621003HCID 18621003, compoundHCID 193754873-acetyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Product 1

HCID 18620727HCID 18620727, compound

Procedure

Using 5-(1-acetyl-4-piperidinyl)valeric acid and 3-acetyl-2,3,4,5-tetrahydro-1H-3-benzazepine, the procedure of Example 23-1 was otherewise repeated to provide the title compound as colorless oil.

Sources & evidence

ORD record
ord-d4db152cb5c1449796d01aed907c6f50
Source dataset
uspto-grants-2003_03
Patent number
US06534496B1

Reaction notes

Loading…