Methyl iodide → HCID 11116940, compound

HRID 1861900Notes

Reaction equation

C([O:5][C:6](=[O:17])[CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([N+:14]([O-:16])=[O:15])[CH:9]=1)(C)(C)C.[CH3:18]I>>[N+:14]([C:10]1[CH:9]=[C:8]([CH:7]([CH3:18])[C:6]([OH:5])=[O:17])[CH:13]=[CH:12][CH:11]=1)([O-:16])=[O:15]

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 18321636HCID 18321636, compound

Product 1

HCID 11116940HCID 11116940, compound

Procedure

Using 3-nitrophenylacetic acid t-butyl ester as a starting material and methyl iodide (1 eq.) as a reagent, the same procedures of Examples 1a and 1b gave 2-(3-nitrophenyl)propionic acid.

Sources & evidence

ORD record: ord-156252c19add44fc868f4c71c76c5480
Source dataset: uspto-grants-2003_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06534546B1

Reaction notes

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