Methyl iodide → HCID 178503982, compound

HRID 1861931Notes

Reaction equation

HRID 1861931 reaction equation
[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1([C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([NH:18][C:19]([NH2:21])=[S:20])[CH:13]=2)[CH2:11][CH2:10][CH2:9]1)([CH3:4])([CH3:3])[CH3:2].[CH3:23]I>>[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1([C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([NH:18][C:19](=[NH:21])[S:20][CH3:23])[CH:13]=2)[CH2:11][CH2:10][CH2:9]1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 22981118HCID 22981118, compound

Product 1

HCID 178503982HCID 178503982, compoundYield 96%

Procedure

Using the compound obtained in Example 158 as a starting material and also using methyl iodide as a reagent, reaction was performed as in Example 29 to give 150 mg of the titled compound (yield, 96%).

Workup

  1. customreaction

Sources & evidence

ORD record
ord-3d9ac3bf7fc9427eb65e8c8936dcccc2
Source dataset
uspto-grants-2003_03
Patent number
US06534546B1

Reaction notes

Loading…