N-Methylethylamine → HCID 22981227, compound

HRID 1861944Notes

Reaction equation

[C:1]([O:5][C:6]([N:8]([C:20]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:21])[CH2:9][C:10]1[CH:15]=[C:14]([N+:16]([O-:18])=[O:17])[CH:13]=[CH:12][C:11]=1F)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:27]([NH:29][CH3:30])[CH3:28]>>[C:1]([O:5][C:6]([N:8]([C:20]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:21])[CH2:9][C:10]1[CH:15]=[C:14]([N+:16]([O-:18])=[O:17])[CH:13]=[CH:12][C:11]=1[N:29]([CH2:27][CH3:28])[CH3:30])=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 12219N-Methylethylamine

HCID 22981229HCID 22981229, compound

Product 1

HCID 22981227HCID 22981227, compoundYield 42%

Procedure

Using the compound obtained in Example 263 as a starting material and also using ethylmethylamine as a reagent, the same procedure of Example 264 gave the titled compound (yield, 42%).

Sources & evidence

ORD record: ord-1fc7d8540ad44e1e9aaad1089e01e996
Source dataset: uspto-grants-2003_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06534546B1

Reaction notes

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