Methyl iodide → HCID 22980953, compound

HRID 1861949Notes

Reaction equation

[C:1]1([CH:7]([O:14][C:15](=[O:28])[CH2:16][C:17]2[CH:22]=[C:21]([N+:23]([O-:25])=[O:24])[CH:20]=[CH:19][C:18]=2[O:26][CH3:27])[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:29]I>>[C:1]1([CH:7]([O:14][C:15](=[O:28])[CH:16]([C:17]2[CH:22]=[C:21]([N+:23]([O-:25])=[O:24])[CH:20]=[CH:19][C:18]=2[O:26][CH3:27])[CH3:29])[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 22980952HCID 22980952, compound

Product 1

HCID 22980953HCID 22980953, compoundYield 46%

Procedure

Using the compound obtained in Example 342 as a starting material and also using methyl iodide (1 eq.) as a reagent, the same procedure of Example 1a gave the titled compound (yield, 46%).

Sources & evidence

ORD record: ord-7b78b8681dd94b74b0388ca417b4b15d
Source dataset: uspto-grants-2003_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06534546B1

Reaction notes

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