HCID 22981206, compound → HCID 17913030, compound

HRID 1861965Notes

Reaction equation

HRID 1861965 reaction equation
[C:1]([O:5][C:6]([N:8]([C:20]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:21])[CH2:9][C:10]1[CH:15]=[C:14]([N+:16]([O-])=O)[CH:13]=[CH:12][C:11]=1[Cl:19])=[O:7])([CH3:4])([CH3:3])[CH3:2]>[Ni]>[C:23]([O:22][C:20]([N:8]([C:6]([O:5][C:1]([CH3:4])([CH3:3])[CH3:2])=[O:7])[CH2:9][C:10]1[CH:15]=[C:14]([NH2:16])[CH:13]=[CH:12][C:11]=1[Cl:19])=[O:21])([CH3:26])([CH3:25])[CH3:24]

Participants

3

Reactant 1

HCID 22981206HCID 22981206, compound

Product 1

HCID 17913030HCID 17913030, compoundYield 98%

Reagents, catalysts & solvents 1

HCID 935NickelCatalyst

Procedure

Using the compound obtained in Example 554 as a starting material and also using Raney nickel as a catalyst, the same procedure of Example 2 gave 3.17 g of the titled compound (yield, 98%).

Sources & evidence

ORD record
ord-920469bc58ca4278936f6f808987d380
Source dataset
uspto-grants-2003_03
Patent number
US06534546B1

Reaction notes

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