HCID 10947469, compound → HCID 11033897, compound

Participants

Reaction Steps

2-(3-tert-Butyldimethylsilyloxyphenyl)nitrobenzene from Step C, (11.94 g, 36.24 mmol) was dissolved in EtOH (250 mL) and EtOAc (250 mL), degassed with argon and Pd/C (1.19 g, 10 wt %) was added. The vessel was subjected to H2 (1 atm) while vigorously stirring for 2.5 hour. The reaction was filtered through a celite pad and concentrated in vacuo, to yield the above-titled compound.

Provenance & Evidence