HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18619274, compound → HCID 18619216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18619274 | HCID 18619274 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18619216 | HCID 18619216 | 95% |
Reaction Steps
A mixture of 0.9 g of 5-benzyloxy-4-(methoxycarbonyl)methoxypyrimidine, 10% palladium/carbon and ethyl acetate was stirred for 3 hours at room temperature under hydrogen atmosphere. The reaction system was purged with nitrogen, then, the reaction solution was filtrated through Celite, and the filtrate was concentrated to obtain 0.574 g of 5-hydroxy-4-(methoxycarbonyl)methoxypyrimidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537948B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-58ebe2121bf243a9ad3a7de95fb5fff0 |
| Source note | uspto-grants-2003_03 |