5-Nitrosalicylaldehyde → HCID 135494205, compound

HRID 1862381Notes

Reaction equation

HRID 1862381 reaction equation
[CH3:1][C:2]1([CH3:10])[CH2:7][CH2:6][C:5](=O)[CH2:4][C:3]1=[O:9].[OH:11][C:12]1[CH:19]=[CH:18][C:17]([N+:20]([O-:22])=[O:21])=[CH:16][C:13]=1[CH:14]=O.[NH2:23][C:24]1[CH:28]=[CH:27][NH:26][N:25]=1>>[OH:11][C:12]1[CH:19]=[CH:18][C:17]([N+:20]([O-:22])=[O:21])=[CH:16][C:13]=1[CH:14]1[C:4]2[C:3](=[O:9])[C:2]([CH3:10])([CH3:1])[CH2:7][CH2:6][C:5]=2[NH:23][C:24]2=[CH:28][CH:27]=[N:26][N:25]12

Participants

4

Reactant 3

HCID 668085-NitrosalicylaldehydeHCID 1363601,3-Cyclohexanedione, 4,4-dimethyl-HCID 178418806HCID 178418806, compound

Product 1

HCID 135494205HCID 135494205, compound

Procedure

4,4-Dimethyl-1,3-cyclohexanedione, 2-hydroxy-5-nitrobenzaldehyde and 3-aminopyrazole were processed as described in General Procedure A to provide the title compound.

Sources & evidence

ORD record
ord-68ac64c577464eb1813fc4b4d41169ed
Source dataset
uspto-grants-2003_03
Patent number
US06538000B1

Reaction notes

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