2-(Tributylstannyl)furan → HCID 135529504, compound

HRID 1862387Notes

Reaction equation

HRID 1862387 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]2[C:18]3[C:17](=[O:19])[CH2:16][CH2:15][CH2:14][C:13]=3[NH:12][C:11]3=[CH:20][CH:21]=[N:22][N:10]23)[CH:5]=[CH:6][C:7]=1[Cl:8].C([Sn](CCCC)(CCCC)[C:28]1[O:29][CH:30]=[CH:31][CH:32]=1)CCC>C1C=CC([P]([Pd]([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]2[C:18]3[C:17](=[O:19])[CH2:16][CH2:15][CH2:14][C:13]=3[NH:12][C:11]3=[C:20]([C:28]4[O:29][CH:30]=[CH:31][CH:32]=4)[CH:21]=[N:22][N:10]23)[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

4

Reactant 2

HCID 43936882-(Tributylstannyl)furanHCID 135494158HCID 135494158, compound

Product 1

HCID 135529504HCID 135529504, compound

Reagents, catalysts & solvents 1

HCID 178418397HCID 178418397, compoundCatalyst

Procedure

The product from Example 6, tetrakis(triphenylphosphine)palladium(0) (0.11 g) and 2-tributylstannylfuran were processed as described in Example 51 to provide the title compound.

Sources & evidence

ORD record
ord-72ae8d2aa7e0461f887df94131559c95
Source dataset
uspto-grants-2003_03
Patent number
US06538000B1

Reaction notes

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