Potassium Carbonate → HCID 10271110, compound

Participants

Reaction Steps

The product from Example 32A (0.09 g) and potassium carbonate(0.03 g) in methanol (10 mL) were stirred at ambient temperature for 1 hour. The solvent was evaporated under reduced pressure and the obtained residue was chromatographed on silica gel eluting with 10% EtOH/CH2Cl2 to provide 0.04 g of the title compound. 1H NMR (300 MHz, DMSO-d6) δ 3.49 (s, 3H),4.76 (s, 1H),4.9 (q, 2H), 7.23 (m, 2H), 7.42 (dd, 1H), 9.51 (bs, 1H), 9.78 (s, 1H)

Provenance & Evidence