HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12045570, compound → HCID 10207643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12045570 | HCID 12045570 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10207643 | HCID 10207643 | 83.9% |
Reaction Steps
(2S)-1-(4-{[tert-butyl(diphenyl)silyl]oxy}phenoxy)-3-({4-[2-(4-ethylphenyl)-3H-imidazo[4,5-b]pyridin-3-yl]phenethyl}amino)-2-propanol (0.13 g, 0.174 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 2% triethylamine) to give the title compound (0.074 g, 0.146 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-0e93a5e7110346d3a1aca1ab9f01b485 |
| Source note | uspto-grants-2003_03 |