HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12045571, compound → HCID 12045568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12045571 | HCID 12045571 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 12045568 | HCID 12045568 | 93.4% |
Reaction Steps
(2S)-1-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-3-({4-[2-(4-cyclohexylphenyl)-3H-imidazo[4,5-b]pyridin-3-yl]phenethyl}amino)-2-propanol (0.317 g, 0.396 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.21 g, 0.37 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-7784f60ed57e49b59447b769a1195e7a |
| Source note | uspto-grants-2003_03 |