HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70007818, compound → HCID 18619663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70007818 | HCID 70007818 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 18619663 | HCID 18619663 | 62% |
Reaction Steps
(2S)-1-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-3-[(4-{2-[2-chloro-4-(3-methyl-1H-pyrazol-1-yl)phenyl]-3H-imidazo[4,5-b]pyridin-3-yl}phenethyl)amino]-2-propanol (0.18 g, 0.216 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.08 g, 0.134 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-d0281eefaf4043d888d08f3430e0a64e |
| Source note | uspto-grants-2003_03 |