Triethylamine → HCID 20393504, compound

Participants

Reaction Conditions

Reaction Steps

To a solution containing 2.9 g (0.01 mole) of the amine prepared in Example 4 (b), and 1.0 g (0.01 mole) of triethylamine in 50 ml of tetrahydrofuran was added dropwise 1.7 g (0.01 mole) of 1-butylcyclopropanecarboxylic acid chloride. The mixture was stirred and heated at 60° C. for 0.5 hour, poured into ice water and extracted with ether. The ether extract was dried and concentrated under reduced pressure. The residual yellow syrup was crystallized from hexane to give 3.3 g (80%) of product as a tan solid, m.p. 104°-106° C.

Provenance & Evidence