HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Cresol → HCID 178512375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178425733 | HCID 178425733 | — |
| Reactant | HCID 178478695 | HCID 178478695 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178512375 | HCID 178512375 | — |
Reaction Steps
6.2 g. (0.031 mole) of 4-(3-aminopropyl)imidazole dihydrochloride is converted to the free base using NaOH. The free base is combined with 5.4 g. (0.031 mole) of O-m-tolyl-N-cyanoisourea in 100 ml. isopropanol. This mixture is refluxed for 3 hours. The mixture is then cooled to room temperature, filtered to remove insoluble material and the solvent is evaporated to obtain a cloudy oil of the product mixed with m-cresol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04166860 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-d8bf31a0bc354f4baaf6a9481cfa65d1 |
| Source note | uspto-grants-1979_09 |