HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 2-(3-Morpholin-4-YL-propoxy)-benzaldehyde | HCID 13795260 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20394050 | 76.5% |
Reaction Steps
2-[3-(4-Morpholinyl)propoxy]benzaldehyde (31.7 g) is reacted with 15.8 g of phenethylamine in 130 ml of toluene following the procedure described in Example 1A to yield 34.3 g of product as an oil, boiling point 215°-219° C. at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04166907 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-4b8d14bee93647818e3afcd017e9a8f2 |
| Source note | uspto-grants-1979_09 |