Glycol diglycidyl ether → HCID 20393562, compound

Participants

Reaction Steps

A mixture of 6.4 g of 4-butylamino-2,2,6,6-tetramethylpiperidine and 2.6 g of ethylene glycol bis(2,3-epoxypropyl)ether in 50 ml of methanol was refluxed, with stirring for 5 hours. At the end of this time, the solvent was removed from the reaction mixture by evaporation under reduced pressure and then the residue was recrystallized from n-hexane, giving the desired compound in the form of white crystals melting at 81°-83° C. and boiling at 258°-262° C. at 0.06 mmHg.

Provenance & Evidence