HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrolein → HCID 612677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrolein | HCID 6562 | — |
| Reactant | 4-Methoxy-2-nitroaniline | HCID 66793 | — |
| Product | HCID 612677 | HCID 612677 | 50% |
Reaction Steps
4-Amino-3-nitroanisole was subjected to a Skraup reaction with 90% methacrolein at 110° to afford a 50% yield of 6-methoxy-3-methyl-8-nitroquinoline. The compound crystallized from ethyl acetate as a yellow solid, mp 173°-175°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04167638 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-3e8bfeaea5e0421ebd7b5ef292150cd8 |
| Source note | uspto-grants-1979_09 |