1-Butanol → Butyl chloroacetate

HRID 1863139Notes

Reaction equation

[Cl:1][CH2:2][C:3]([OH:5])=[O:4].[CH2:6](O)[CH2:7][CH2:8][CH3:9]>>[Cl:1][CH2:2][C:3]([O:5][CH2:6][CH2:7][CH2:8][CH3:9])=[O:4]

Participants

Reactant 2

HCID 2631-Butanol

HCID 300Chloroacetic Acid

Product 1

HCID 11530Butyl chloroacetate

Procedure

Following the procedure described in Examples 1 and 2, but heating while stirring for 4 hours to 105° a mixture comprising of 181 parts of butanol and 189 parts of chloroacetic acid, there is obtained butyl chloroacetate; nD20 =1,428.

Workup

temperatureheating

Sources & evidence

ORD record: ord-16623a4ca0d44270b7da9ef587ba636e
Source dataset: uspto-grants-1979_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04168142

Reaction notes

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