HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 20392602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 20392615 | HCID 20392615 | — |
| Catalyst | Hydrogen Bromide | HCID 260 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 20392602 | HCID 20392602 | — |
Reaction Steps
To a suspension of 1.6 g of methyl α-[p-(p-methylsulfonylphenoxy)phenyl]acetate in 25 ml of carbon tetrachloride is added 0.98 g of N-bromosuccinimide and 1 drop of 48% HBr. The mixture is stirred and refluxed for 19.5 hours and 10 mg of benzoyl peroxide is added. The mixture is refluxed for 3 hours and 1/2 inch of 22 gauge nichrome wire is added. After refluxing an additional 18 hours the solvent is removed under vacuum to give the product as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168385 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-11093dbb807447a7a172872364d88084 |
| Source note | uspto-grants-1979_09 |